A Comprehensive Treatise Inorganic and Theoretical Chemistry by Mellor J.W. PDF

By Mellor J.W.

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336 1H, 13C 21 Spectrosc. Prop. Inorg. Organomet. 344 1H and 31P{1H} NMR spectra for (67), where M ¼ Rh or Ir, were reported. 348 31P NMR data were able to discriminate between enantiomers 22 Spectrosc. Prop. Inorg. Organomet. 353 2-D NMR experiments enabled a full characterisation of 4 isomers of [Ir(H)2{(S)-(R)L}(L 0 )]1, where L ¼ S-1-[(R-2-diphenylphosphanyl)ferrocenyl] ethyldi(3,5-xylyl)phosphane; L 0 ¼2,6-dimethylphenyl-1 0 -methyl-2 0 -methoxy354 1 31 ethylimine. 361 NMR data have also been reported for: Co3(CO)6[m2,Z2,Z1-C(Ph) C¼C(PPh2C(O)SC(O)](m2-PPh2) (31P);362 Co3(CO)9[m3-CCO2CH2CCH{Co4 (CO)10}] (1H);363 substituted m3-carbido-capped tricobalt carbonyl clusters (1H, 13C);364 Co(III) complexes of NH3, en, 1,2-propylenediamine or 1,2-cyclohexanediamine (1H, 13C, 59Co);365 [Co(CO)3(L)]À (L ¼ N,N-diethyl1,2-ethanediamine, N,N-bis(2-chloroethyl)-1,2-ethanediamine and related) (1H, 13C{1H});366 cis-[Co(en)2(N3)2]SCN (1H, 13C);367 (70), where R ¼ n-octyl, n-dodecyl, n-hexadecyl (1H, 13C);368 [CH2ClCo(tmsalen)]2, 3+ NH NH + H NH Co Cy P Ph3P Ir Co t Bu NH NH NH PPh3 (69) (70) R 23 Spectrosc.

Prop. Inorg. Organomet. g. n(thf) Si O Cl (150) (151) N Si Si O O Si Si O O Si O Si O O Si O Si O Si (152) 43 Spectrosc. Prop. Inorg. Organomet. 3 Germanium Compounds. 4 Tin Compounds. 735 1 H and 119Sn NMR spectra of [H2B(im)2]RnSnCl4ÀnÀ1, where[H2B(im)2]À ¼ 44 Spectrosc. Prop. Inorg. Organomet. 746 NMR data were also reported for: Me3SnX, where X ¼ OTeF5, N(SO2F)2, N(SO2CF3)2 (1H, 13C, 19F, 119Sn, 125Te);747 R3Sn(ceph), R2Sn(OH)(ceph) (R ¼ Me, nBu; Hceph ¼ deacetoxy-cephalosporin antiobiotic) (1H, 13C, 119Sn);748 RnSn(OSO2C6H4CH3-4)4Àn (n ¼ 2, 3; R ¼ Et, nPr, nBu);749 (Ph3Sn)2(m-oxalato) (119Sn);750 (159) and related Si and Ge species (1H, 13C, 11B, 29Si, 119Sn);751 R3SnL, R2SnL2 (R ¼ Bu, Ph, PhCH2, n-C8H17; HL ¼ 2-[(2,3-dimethylphenyl)amino]benzoic acid) (1H, 13C, 119Sn);752 nBu3Sn(L) (L ¼ C6H4SEt-2, 45 Spectrosc.

585 1H and 31P NMR specta were used to study interaction of tris3-pyridylphosphine and mesophenyl zinc(II) porphyrin in CDCl3 solution. e. 596 The P31{1H} NMR spectra of Pt(C-P)(mO2CR)2HgX, where C–P ¼ –CH2C6H4P(o-tolyl)2-kC,P, R ¼ CH3, CF3, X ¼ Cl, Br, I, all show 199Hg-P coupling consistent with a strong Pt–Hg bond in 37 Spectrosc. Prop. Inorg. Organomet. g. 13 Compounds of Group 13. 1 Boranes and Heteroboranes. 617 38 Spectrosc. Prop. Inorg. Organomet. 2 Other Boron Compounds. 620 1H, 11B, 13C and 29Si NMR data for (132) (R ¼ Me, R 0 ¼ SiMe3, Ph, Bu; R ¼ iPr, R 0 ¼ SiMe3, SiHPh2, Fc, are consistent with the presence of an Si–H .

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