By A. Furstner
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Additional resources for Active Metals [chemistry]
These functionalized organocopper reagents undergo many of the same reactions as other organocopper species, including cross-coupling reactions with acid chlorides, 1,6conjugate additions with a$-unsaturated carbonyl compounds, and intermolecular and intramolccular epoxide-opening reactions. 2 Background to the Development of Rieke Copper Initial attempts to prepare highly reactive copper in our laboratories were only partially successful due to rapid sintering of thc finely divided copper .
Although this copper was found to be more reactivc than the ordinary copper bronze used in the traditional Ullman reaction. it lacked thc rcactivity necessary to react with the majority of organic halidcs. When compared with other metals produccd by the Rieke method of metal activation, copper suffers from the disadvantage of sintering into larger particlcs, thereby reducing its reactivity. It was apparent that the main difficulty associated with the copper metal \intering was the cxceptionally long reduction time.
5]decan-2-one(6) was obtained. Table 1-7 shows representative spiro-ylactones that have been prepared in this way. We have recently reported an extension of this methodology in the production of spiro-d-lactones . Much work has been done to elucidate novel synthetic routes for these types of molecules . In particular, d-substituted d-lactones have recently attracted considerable attention, mainly because molecules of this class include many natural products that exhibit significant biological activity .
Active Metals [chemistry] by A. Furstner