Download PDF by Daisuke Shindo, Hiraga Kenji: High-Resolution Electron Microscopy for Materials Science

By Daisuke Shindo, Hiraga Kenji

ISBN-10: 4431684220

ISBN-13: 9784431684220

ISBN-10: 4431702342

ISBN-13: 9784431702344

High-resolution electron microscopy (HREM) has turn into a strongest technique for investigating the inner constitution of fabrics on an atomic scale of round 0.1 nm. The authors truly clarify either the idea and perform of HREM for fabrics technology. as well as a primary formula of the imaging strategy of HREM, there's distinct clarification of picture simulationindispensable for interpretation of high-resolution photographs. crucial info on applicable imaging stipulations for gazing lattice pictures and constitution photographs is gifted, and techniques for extracting structural info from those observations are sincerely proven, together with examples in complex fabrics. Dislocations, interfaces, and surfaces are handled, and fabrics comparable to composite ceramics, high-Tc superconductors, and quasicrystals also are thought of. integrated are sections at the most recent tools and strategies, equivalent to the imaging plate and quantitative HREM.

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Additional info for High-Resolution Electron Microscopy for Materials Science

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50 3. Application of High-Resolution Electron Microscopy Fig. 9. Lattice image of silicon with the incident electron beam perpendicular to both partial dislocation lines, and a stacking fault between them. Specimen: Si; Preparation: chemical polishing (HNOi HF); Observation: 200 k V EM, [111] incidence. Remarks: Lattice fringes are observed only at the region corresponding to a stacking fault. 33 nm, corresponding to forbidden reflections. Kinks are located by tracing the edge of the stacking faults.

3. Lattice image of a dissociated dislocation in deformed silicon. Specimen: Si; Preparation: chemical polishing (HNO/HF); Observation: 1000kY EM. Remark: At the ends of the stacking fault there are 30° (A) and 90° (B) partial dislocations 44 Fig. 4. Lattice image of a faulted dipole in silicon. Specimen: Si; Preparation: chemical polishing (HNOiHF); Observation: lOOOkV EM. Remark: The Z-type faulted dipole is formed from three stacking faults. This faulted dipole results from the interaction of two dissociated dislocations moving in the crystal, as indicated in the inset 45 46 3.

The image indicates that a 60° perfect dislocation dissociates into 30° (A) and 90° (B) partial dislocations. 4mJ m- 2 [5, 6]. The high-resolution image of silicon in Fig. 4 shows a characteristic lattice defect, a so-called Ztype faulted dipole. As shown in the inset, this defect forms when two dissociated moving dislocations interact each other and connect through the stacking fault AB. Extra half-planes exist above and below the stacking faults being at the top and bottom of the faulted dipole, respectively.

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High-Resolution Electron Microscopy for Materials Science by Daisuke Shindo, Hiraga Kenji

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